Inzira rusange yo gukuramo icyiciro gikomeye niyi ikurikira:

1. Uburyo butandukanye bwo gukuramo icyiciro gikomeye cyo gukuramo cartridge ikoresha imashanyarazi itandukanye:

. Birashoboka kandi koza hamwe na solge ikomeye (nka hexane) mbere yo koza methanol kugirango ikureho umwanda wamamajwe kuri adsorbent no kwivanga kwabo.

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. iyo ikoreshejwe kuburugero rwumuti wa polar, irashobora gukaraba hamwe namazi yumuti ukomoka kumazi Nyuma yo gukaraba, kwoza hamwe nigisubizo cyamazi cyagaciro ka pH gikwiye kandi kirimo imyunyu ngugu hamwe numunyu.

Kugirango ugumane sorbent muri karitsiye ya SPE nyuma yo gukora na mbere yo kongeramo icyitegererezo, hafi ml 1 ya solvent yo gukora igomba kubikwa kuri sorbent nyuma yo gukora.

2. Icyitegererezo cyo gupakira: Suka amazi meza cyangwa yashonze icyitegererezo muri karitsiye ikora yo gukuramo icyiciro, hanyuma ukoreshe vacuum, igitutu cyangwa centrifugation kugirango icyitegererezo cyinjire muri adsorbent.

3. Gukaraba no guhanagura: Nyuma yicyitegererezo cyinjiye muri adsorbent hanyuma uruganda rugenewe rwamamajwe, uruganda rwabigizemo uruhare rudakomeye rushobora gukaraba hamwe n’umuti udakomeye, hanyuma uruganda rugenewe rushobora gutorwa hamwe nigisubizo gikomeye kandi cyegeranijwe. . Kwoza no Kwiyuhagira Nkuko byasobanuwe mbere, umuhanga cyangwa umuhanga ashobora kunyuzwa muri adsorbent hakoreshejwe vacuum, igitutu cyangwa centrifugation.

Niba adsorbent yaratoranijwe kugirango igire intege nke cyangwa ntizishobora kwinjizwa murwego rwintego hamwe na adsorption ikomeye kubivangavanga, uruganda rwintego narwo rushobora kwozwa no gukusanywa mbere, mugihe uruvangitirane rugumanye (adsorption). ) kuri adsorbent, byombi biratandukanye. Mu bihe byinshi, intego yibikoresho igumishwa kuri adsorbent, hanyuma ikarangizwa hamwe nigisubizo gikomeye, kikaba cyiza cyane mugusukura icyitegererezo.